- all spectroscopy and spectrometry videos
- day 1 pre-lab
- day 2 pre-lab
- day 3 pre-lab
- problem sets and solutions
- MestReNova installation instructions
- additional resources
Lab Safety and Course Policies
Experiment 3: Separation of a Mixture by Acid-Base Extraction
- chemical safety information
- spectral workup instructions
- sample and stock spectra
- frequently asked questions
Experiment 4: Computational Molecular Modeling (WebMO)
Experiment 5: Nucleophilic Substitution Reactions (SN1/SN2)
- chemical safety information
- spectral workup instructions
- sample and stock spectra
- additional reading
- frequently asked questions
Experiment 6: Elimination Reactions (E1/E2)
Experiment 7: Oxidation of 4-tert-Butylcyclohexanol
Experiment 9: Wittig Synthesis of Ethyl Cinnamate
Experiment 10: Stereochemistry of a Carbonyl Reduction
Experiment 11: Electrophilic Aromatic Substitution – Nitration
- chemical safety information
- spectral workup instructions
- sample and stock spectra
- frequently asked questions
Experiment 12: Electrophilic Aromatic Substitution – Acylation
Experiment 13: Grignard Reaction of 1-Fluoro-4-bromobenzene
- chemical safety information
- organometallics pre-lab videos
- sample and stock spectra
- frequently asked questions
Experiment 15: Aerobic Oxidation of an Alcohol Using a Cu/TEMPO Catalyst System
Experiment 22: SNAr Reaction of a Fluorinated Aromatic Compound
- chemical safety information
- recommended reading
- sample and stock spectra
- frequently asked questions
Legacy Experiments:
Experiment 8: Reactions of Nitrogen Functional Groups
Experiment 14: Suzuki Coupling
Experiment 16: Biginelli Synthesis of a Heterocycle
Experiment 17: Aldol Condensation
Experiment 18: Transesterification Catalyzed by an N-Heterocyclic Carbene
Experiment 19: Radical Bromination of Bibenzyl
Experiment 20: Nucleophilic Substitution Reactions (SN1/SN2)
- chemical safety information
- spectral workup instructions
- sample and stock spectra
- additional reading
- frequently asked questions
Experiment 21: Grignard Reaction of Chlorobromobenzene with DMF