Department of Chemistry
College of Letters & Science

Experiment 21: Grignard Reaction of Chlorobromobenzene with DMF

Due Dates:

1 May / 2 May A/B

Chemical Safety Information:

Reagents and Solvents
1-Bromo-4-chlorobenzene DMF hydrochloric acid
magnesium sulfate deuterated chloroform diethyl ether
1,2-dibromoethane Magnesium

 

Organometallic Chemistry Lecture:

CHEM 344 Organometallic Chemistry Lecture (current version, without subtitles)

Chem 344 Organometallics Lecture – Notetaking Slides

Experimental Spectra:

Sample 1H-NMR spectrum of 1-bromo-4-chlorobenzene  (FOR REFERENCE ONLY)

Sample 1H-NMR Grignard Product of 1-bromo-4-chlorobenzene and DMF (Not available for credit)

Stock FID 1H-NMR Grignard Product of 1-bromo-4-chlorobenzene and DMF (available for submission for credit, see laboratory manual for details)

Stock GC-MS spectrum of Grignard Product of 1-bromo-4-chlorobenzene and DMF (available for submission for credit, see laboratory manual for details)

Stock IR spectrum of Grignard Product of 1-bromo-4-chlorobenzene and DMF (available for submission for credit, see laboratory manual for details)